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GCMS sample analysis report for AD29928, Jan 2002

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Laboratory analysis report for environmental sample AD29928 showing GCMS results and surrogate compound recovery rates.

NYC-WTC_000037448–000037456

Folder label: “GCMS X 12/11/01 A 12/16/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\DEC1401\29927.D Vial: 52 Acq On 16 Dec 2001 4:28 pm Operator: 209 GALOS Sample gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 16 17:17 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.04 178 1100 N.D. 34) Anthracene 25.04 178 1100 N.D. 35) Di-n-butylphthalate 27.00 149 20574 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.01 228 3278 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 8109 N.D. 43) Chrysene 33.01 228 3278 N.D. 45) Di-n-Octylphthalate 35.01 149 193 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.10 252 3043 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29927.D GCMS1126.M Wed Jan 30 11:37:24 2002 Page 2

NYC-WTC_000037451

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NYC-WTC_000037451Source: NYC Law Department, mirrored locally

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