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GCMS analysis results for sample AD30011, Jan 2002

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Gas chromatography-mass spectrometry report documenting analysis of sample AD30011 conducted on January 28, 2002.

NYC-WTC_000037314–000037326

Folder label: “GCMS X 12/11/01 A 12/18/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1801\30012.D Vial: 9 Acq On : 18 Dec 2001 11:54 pm Operator: 2 09 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 10:13 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.04 178 475 N.D. 34) Anthracene 25.04 178 475 N.D. 35) Di-n-butylphthalate 27.00 149 10169 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.02 228 4065 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 3915 N.D. 43) Chrysene 33.02 228 4065 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.10 252 4369 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30012.D GCMS1126.M Tue Jan 15 10:15:35 2002 Page 2

NYC-WTC_000037317

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NYC-WTC_000037317Source: NYC Law Department, mirrored locally

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