NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC1401\26320.D Vial: 25
Acq On : 16 Dec 2001 1:54 am Operator: 209 GALOS
Sample : gems scan 12/10 a Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Dec 16 2:43 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update
Response via
DataAcq Meth
:
:
:
Fri Dec 14 12:19:30 2001
Initial Calibration
GCMS1126
2pl exr
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 849952 20.00 ug/1 -0.03
10) Naphthalene-d8 15.28 136 3266156 20.00 ug/1 -0.03
17) Acenaphthene-diO 20.56 164 1656717 20.00 ug/1 -0.02
29) Phenanthrene-dlO 24.97 188 2363976 20.00 ug/1 -0.02
38) Chrysene-dl2 33.00 240 148570'1 20.00 ug/1 -0.03
44) Perylene-dl2 37.10 264 922581 20.00 ug/1 -0.02
System Monitoring Compounds
37) 2,4-DDD 30.05 235 143057 4.18 ug/mL -0 ; 02
Spiked Amount 5.000 Recovery = 83.60%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.20 74 175 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine ' 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 ' 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene ■ 0.00 180 0 N.D.
15) Naphthalene 15.33 128 1218 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 .0 N.D.
24) 2,4-Dinitrotoluene 21.11 165 384 N.D.
25) Diethylphthalate 22.09 149 1081 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 ' 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
26320.D GCMS1126.M Fri Dec 28 12:57:04 2001 Page 1
NYC-WTC_000037106
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