GCMS blank analysis results for sample AD29565, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC14 01\LBD.D Vial: 14 Acq On 15 Dec 2001 3:13 pm Operator: 209 GALOS Sample gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 2.84 ug/1 791409 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW Mol Form. CAS# Qual

1 1,3-Dioxol me, 2-methyl- 000497-26-7 9 88 C4H802 2 N-Ethylformamide 000627-45-2 9 73 C3H7NO 3 Pentane, 3-methoxy­ 036839-67-5 9 102 C6H140 4 1,3 -Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 278 (7.599 min): LBD.D (-) m/ z 73.00100.00% 73

5000 43

87 103 7.20 7.40 7.60 7.80 8.00 3? |, | 50 55 .50 67, 1 TIBBEEn/mm m/ z 43.00 27.06% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902: 1,3-Dioxolane, 2-methyl- 73

5000 43 7.20 7.40 7.60 7.80 8.00 58 m/ z 44.9.5 10.32% 87 • ■ i ■ ■ ' ' i. 27 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73 1 i 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.00 9.61% 44 58

15........J TT1B.BT i ]-i-r-r-r-|-r-r-r-r IT t ... I.... .............. miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- IIt M r l , . i । , , TIIm 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.93% 5000 45

27 33 39. 55 i • ■ ■ ■ i • • ■ ■ । ■ 'i । m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

LBD.D GCMS1126.M Fri Dec 28 13:31:09 2001 Page 1

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