GCMS analysis results for sample AD25946, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\25946.D Vial: 25 Acq On 1 Jan 2002 10:15 am Operator: 209 GALOS Sample gems scan 12/14a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.62 3.78 ug/1 1024920 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 4 Pentane 3-methoxy­ 102 C6H140 036839-67-5 9 Abundance 4 Scan 280 (7.618 mln): 25946.D (-) m/z 72.95 100.00% 73

5000 43 =

3? , 50 55 .61 67, , +-T 87 103 7.20 7.40 7.60 7.80 8.00 11—9————— ■ l ' ‘ I 1 ■ 1 ' l 1 ' ' ' I 1 1 m/z 43.00 33.40% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902:1,3-Dioxolane, 2-methyl- 73 8 5000 43 7.20 7.40 7.60' 7.80 8.00 58 m/z 41.00 11.77% 27 87 i ■ ■ ■ ■ i 1 « > i • • i • • ■ ■ i ■ 1 ■ ■ i • ■ ■ ■ i 1 ■ ■ ■ i ■ • • ■ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- 3b

7.20 7.40 7.60 7.80 8.00 5000 m/z 44.95 11.67%

15 ; I 41 55 70 87 • ■ i ■ ■ • » । ■ i ■ ■ ' 1 i 1 ■ ■ ■ i ■ ■ ■ 1 i ■ ■ ■ ■ I ■ ■ ■ ■ i ■ • ■ ■ i ■ ‘ ■ i ■ ‘ ' I ' 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide —1ddnman3t—atTprTtt 30 7.20 7.40 7.60 7.80 8.00 73 m/z 71.00 6.78% 5000 44 58 15 ----- ■ ■ "li" ■1 i 1 ' i ■ ■ ■ ■ i ■ 1 ■ ' i ■ ■ ' ■ i 1 • ■ ‘ i • • ■ 1 I 1 1 akania . fTT r-r । . . miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

25946.D GCMS1126.M Tue Jan 15 14:46:46 2002 Page 1

NYC-WTC_000018003