GCMS blank analysis results for sample AD29565, Dec 2001

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LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1401\LBD.D Vial: 14 Acq Ori 15 Dec 2001 3:13 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.599 274 278 299 rBV 306777 791409 10.21% 2.042% 2 11.354 682 687 692 rBV 43414 110535 1.43% 0.285% 3 11.436 692 696 705 rVB 44505 126012 1.63% 0.325% 4 11.675 716 722 746 rBV 2273888 5574509 71.93% 14.384% 5 15.274 1109 1114 1135 rBV 3211146 7108738 91.72% 18.343%

6 20.552 1683 1689 1712 rBV 3456128 . 7750167 100.00% 19.998% 7 24.977 2164 2171 2184 rBV2 3174395 7170298 92.52% 18.502% 8 25.124 2184 2187 2198 rVB2 28832 103467 1.34% 0.267% 9 30.054 2718 2724 2732 rBV 422575 885297 11.42% 2.284% 10 33.010 3039 3046 3067 rBV2 2079901 5058394 65.27% 13.052%

11 33.295 3072 3077 3091 rVB 92437 275145 3.55% 0.710% 12 37.105 3484 3492 3516 rBV 1295286 3800770 49.04% 9.807%

Sum of corrected areas: 38754741

LBD.D GCMS1126.M Fri Dec 28 13:30:53 2001

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