GCMS analysis results for sample AD29786, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29786.D Vial: 11 Acq On : 15 Dec 2001 12:18 pm Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 3.89 ug/1 1039910 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 entative ID MW MolForm CAS# Qual

1 N-Ethylfo rmamide 73 C3H7NO 000627-45-2 9 2 Butane, -methoxy-2-methyl - 102 C6H140 000994-05-8 9 3 1,3-Dia olane, 2- (3-bromo-5, 5, 5-tri 352 C10H16BrC13O2 000000-00-0 9 4 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 5 'Abundance Scan 277 (7.591 min): 29786.D (-) m/z 73.00 100.00% 73

5000 43

—34+—56 67 । - 87- 103 7.20 7.40 7.60 7.80 8.00 m/z 43.00 27.13% 'm/z-> 10 20 30 401 50 60 70 80 90 100 110 120 'Abundance #292: N-Ethylformamide I 30 73

5000- —r I 58 7.20 7.40 7.60 7.80 8.00 44 m/z 41.00 10.19%

m/z-> 5 10 20 30 ■ 4— 40 50 60 70 80 90 100 110 120 Abundance #1761: Butane, 2-methoxy-2-methyl- 73 । । I । ’ ' * 1 -pr PI- 7.20 7.40 7.60 7.80 8.00 5000- m/z 45.00 10.11%

A 55 87 i 45 I 27 33 mdnmrmoonopmn -..................... - ' i ■ ' ' ' i ' ' ' ' i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 6.20% 5000 45 ................ 36 l i ' 1 ' ■ i ' ■ • ■ i ■ ■ 1 ■ i ' 1 ■ 55 67 < I • ■ ■ ■ l ■ ■ ■ ■ । • +, ‘I IIT , 109 115TIInn 7.20 7.40 7.60 7.80 ‘ 8.00 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120

29786.D GCMS1126.M Fri Dec 28 13:21:17 2001 Page 1

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