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GCMS calibration table for TCLP method, Dec 2001

Machine-extracted title · confidence 100%

Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 13, 2001.

NYC-WTC_000036944–000036946

Folder label: “GCMS X 12/7/01 A 12/18/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : M:\INSTRU-1\2 09\DATA\DEC13 01\LBA.D Vial: 16 Acq On : 13 Dec 2001 11:32 pm Operator: 209 GALOS Sample : gems scan Y2./1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 8 11:31 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.03 178 541 N.D. 34) Anthracene 25.03 178 541 N.D. 35) Di-n-butylphthalate 26.99 149 26634 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.51 149 693 N.D. 41) Benzo(a)anthracene 33.01 228 5797 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 9218 N.D. 43) Chrysene 33.01 228 5797 N.D. 45) Di-n-Octylphthalate 35.40 149 181 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 4 7) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.11 252 6045 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration LBA.D GCMS1126.M Thu Jan 10 12:40:36 2002 Page 2

NYC-WTC_000036945

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NYC-WTC_000036945Source: NYC Law Department, mirrored locally

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