GCMS analysis results for sample AD29565, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File M:\INSTRU~1\209\DATA\DEC1801\29565.D Vial: 3 Acq On 18 Dec 2001 6:01 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 4.99 ug/1 1162830 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 2 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 3 1,3 -Dioxolane , 2-pentadecyl- 284 C18H36O2 004360-57-0 9 4 Pentane, 3-methoxy-___________ 102 C6H140 036839-67-5 9 Abundance •- Scan 279 (7.603 min): 29565.D (-) m/z 73.0,0 100.00% 73

5000 43 7.20 7.40 7.60 7.80 8.00

m/z--> -l 57 87 103 Ti 1 1 ' ' i ' 20 40 60 80 100 120 140 160 180 200 220 240 260 280 m/ z 43.05 29.07% Abundance #62932: Silane, tetramethyl- 73

5000 7.20 7.40 7.60 7.80 8.00 45 m/z 45.05 11.14% 15 miz—> ' 445960 8088100 I ■ ' ' ' I 20 40 ...................................... 120 140 160 180 200 220 240 260 280 Abundance #292; N-Ethylformamide 30 73 TPTruur 7.20 7.40 7.60 7.80 8.00 5000 m/ z 41.00 9.70% 44 58

15 ,1 ■ ■ । ■' ■ ■ । m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #40191: 1,3-Dioxolane, 2-pentadecyl- 1*/*————/. 73 7.20 7.40 7.60 7.80 8.00 m/z 71.0,0 6.87% 5000 -

43 57 86 99 256 283 . I i < । i p , । f । । i । । [ i r r i । "i i m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 7.20 7.40 7.60 7.80 8.00

29565.D GCMS1126.M Thu Jan 10 12:38:12 2002 Page 1

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