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GCMS analysis comments for sample AD29517 re-analysis required, Jan 2002

Machine-extracted title · confidence 95%

Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.

NYC-WTC_000036656–000036677

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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Scanned page image, NYC-WTC_000036677
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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: 209 GALOS Date Acquired: 4 Jan 2002 2:10 am Data File: C:\HPCHEM\1\DATA\JAN0302\29517.D Name: gems scan Mise: Method: C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

3 - Pentanol , 3 - me t hyl 7.47 2.4 ug/1 1191500 ISTD01 11.53 10032600 20.0 2-Prepanone , 1,1,1-t 7.61 0.4 ug/1 208030 ISTD01 11.53 10032600 20.0 Cyclotetrasiloxane, 10.99 1.6 ug/1 799095 ISTD01 11.53 10032600 20.0 2-Propanol , l-(2-met 11.20 2.0 ug/1 1004440 ISTD01 11.53 10032600 20.0 2-Propanol, l-(2-met 11.27 2.3 ug/1 1159190 ISTDOl 11.53 10032600 20.0 Cyclopentasiloxane, 14.17 2.1 ug/1 1130850 ISTD02 15.12 10794900 20.0 Cyclohexasiloxane, d 17.31 2.6 ug/1 1417400 ISTD02 15.12 10794900 20.0 Trisilexane , 1,1,1,5 20.13 1.6 ug/1 929209 ISTD03 20.39 11347200 20.0 Benzoic acid, 4-etho 20.85 0.7 ug/1 372255 ISTD03 20.39 11347200 20.0 N-(Tri fluoracetyl)-O 22.63 1.1 ug/1 598077 ISTD04 24.81 11239600 20.0 3 - Isopropoxy- 1,1, 1,7 26.74 0.5 ug/1 282769 ISTD04 24.81 11239600 20.0 3 - Isopropoxy- 1,1,1,7 30.09 0.5 ug/1 190860 ISTD05 32.84 7451820 20.0 1 - Monolino leoylglyce 31.56 0.4 ug/1 157328 ISTD05 32.84 7451820 20.0 Trisil oxane , 1,1,1,5 32.93 0.6 ug/1 238016 ISTD05 32.84 7451820 20.0

29517.D GCMSL126.M Tue Jan 08 12:20:58 2002

NYC-WTC_000036677

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NYC-WTC_000036677Source: NYC Law Department, mirrored locally

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