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GCMS analysis results for sample AD30985, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.

NYC-WTC_000018262–000018285

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: 209 GALOS Date Acquired: 2 Jan 2002 1:45 am Data File: C:\HPCHEM\l\DATA\DEC3101\30985.D Name: gems scan 12/19 Mise: Method: C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

3—Pentanol,—3- methyl 7.61 3.4 ug/1 917358 ISTD01 11.67 5350240 20.0 Cyclotetrasiloxane, 11.13 3.2 ug/1 864282 ISTD01 11.67 5350240 20.0 Gyclopentasi l oxane, 14.30 6.9 ug/1 2329340 ISTD02 15.28 6724180 20.0 Cya lohexas il oxane, d 17.45 10.3 ug/1 3467340 ISTD02 15.28 6724180 20.0 2 -Propanone, 1-(1-me 18.16 0.6 ug/1 214054 ISTD03 20.56 7387620 20.0 3 - Isopropoxy-1,1,1,7 20.27 6.7 ug/1 2484290 ISTD03 20.56 7387620 20.0 Benzoic acid, 4 - etho 21.06 1.3 ug/1 489196 ISTD03 20.56 7387620 20.0 Benzeneethanamine, N 22.79 3.9 ug/1 1586800 ISTD04 24.98 8150300 20.0 1-Monolinoleoylglyce 26.89 1.9 ug/1 774406 ISTD04 24.98 8150300 20.0 1-Monol inolcoylglyce 28.65 1.5 ug/1 612351 ISTD04 24.98 8150300 20.0 1,1,15+77,7 -Hept am 30.25 2.0 ug/1 568765 ISTD05 33.02 5630060 20.0 1Monolinoleoylglyce 31.72 2.0 ug/1 553466 ISTD05 33.02 5630060 20.0 1-Monol inoleoyl glyc e 34.37 1.3 ug/1 373890 ISTD05 33.02 5630060 20.0 Decanedioic acid, bi 35.58 25.5 ug/1 4400830 ISTD06 37.12 3456200 20.0 Eri si lexane, 1,1,1,5 36.71 0.9 ug/1 150889 ISTD06 37.12 3456200 20.0 Mercaptoacetic acid, 38.01 0.5 ug/1 84166 ISTD06 37.12 3456200 20.0

30985.D GCMS1126.M Wed Jan 23 08:58:17 2002

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NYC-WTC_000018285Source: NYC Law Department, mirrored locally

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