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GCMS blank analysis results, Jan 2002

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Laboratory report documenting GCMS blank analysis for organic compounds conducted on January 4, 2002, showing results below detection limits.

NYC-WTC_000036503–000036512

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1301\LB.D Vial: 4 Acq On : 13 Dec 2001 12:47 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 20 10:47 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.04 178 541 N.D. 34) Anthracene 25.04 178 541 N.D. 35) Di-n-butylphthalate 27.00 149 15134 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.50 149 7002 N.D. 41) Benzo(a)anthracene 33.01 228 4839 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 70920 0.66 ug/1 98 43) Chrysene 33.08 228 542 N.D. 45) Di-n-Octylphthalate 35.04 149 2038 N.D. 46) Benzo(b)fluoranthene 36.07 252 166 N.D. . 47) Benzo(k)fluoranthene 36.14 252 697 N.D. 48) Benzo(a)pyrene 36.93 252 333 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo (g; h, i) perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS1126.M Fri Dec 21 12:59:27 2001 Page 2

NYC-WTC_000036505

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NYC-WTC_000036505Source: NYC Law Department, mirrored locally

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