NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC1201\29461.D Vial: 18
Acq On : 12 Dec 2001 7:35 pm Operator: 209 GALOS
Sample : gc/ms scan 12/5 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Dec 20 10:37 2001 Quant Results File: GCMS1126.RES
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title 209 625/TCLP calibration table
Last Update Wed Nov 28 15:06:24 2001
Response via Initial Calibration
DataAcq Meth GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 969325 20.00 ug/1 - 0.03
10) Naphthalene-d8 15.28 136 3707286 20.00 ug/1 -0.03
17) Acenaphthene-diO 20.55 164 1857120 20.00 ug/1 -0.02
29) Phenanthrene-diO 24.97 188 2659601 20.00 ug/1 -0.02
38) Chrysene-dl2 33.01 240 1721050 20.00 ug/1 -0.02
44) Perylene-dl2 37.10 264 1166891 20.00 ug/1 -0.02
System Monitoring Compounds
37) 2,4-DDD 30.05 235 117369 3.71 ug/mL -0.02
Spiked Amount 5.000 Recovery = 74.20%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 18 0 0 N.D.
15) Naphthalene 15.33 128 1429 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.26 165 425 N.D.
25) Diethylphthalate 22.08 149 691 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
29461.D GCMS1126.M Fri Dec 21 12:44:45 2001 Page 1
NYC-WTC_000036471
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