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GCMS analysis results sample AD29458, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29458 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036436–000036446

Folder label: “GCMS X 12/5/01 A 12/12/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1201\29458.D Vial: 30 Acq On : 13 Dec 2001 6:16 am Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 20 10:43 2001 Quant Results File: GCMS1126.RES

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Last Update Wed Nov 28 15:06:24 2001 Response via Initial Calibration DataAcq Meth GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.98 178 839 N.D. 34) Anthracene 24.98 178 839 N.D. 35) Di-n-butylphthalate 27.00 149 4897 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.01 228 4235 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 12881 N.D. 43) Chrysene 33.01 228 4235 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.10 252 4592 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29458.D GCMS1126.M Fri Dec 21 12:55:38 2001 Page 2

NYC-WTC_000036439

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NYC-WTC_000036439Source: NYC Law Department, mirrored locally

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