GCMS analysis results sample AD29345, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29345 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036414–000036424

Folder label: “GCMS X 12/5/01 A 12/12/01”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Pile : C:\HPCHEM\1\DATA\DEC1201\29345.D Vial: 21 / n : 12 Dec 2001 10:30 pm Operator: 209 GALOS Le gc/ms scan 12/5 Inst : GC/MS 209 Mi. Multiplr: 1.00 MS integration Params: RTEINT.P Quant Time: Dec 20 10:38 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Conc Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11..68 152 921788 20.00 ug/l -0.02 10) Naphthalene-d8 15.27 136 3517263 20.00 ug/l -0.03 17) Acenaphthene-d10 20.55 164 1712444 20.00 ug/l -0.02 29) Phenanthrene-d10 24.97 188 2457264 20.00 ug/l -0.02 38) Chrysene-d12 33.01 240 1510154 20.00 ug/1 -0.02 44) Perylene-d12 37.10 264 978137 20.00 ug/l -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 118326 4.04 ug/mL -0.02 Spiked Amount 5.000 Recovery = 80.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146' 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(l-Chloropropan 0:00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 . 180 0 N.D. 15) Naphthalene 15.34 128 828 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 ' N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.07 165 198 N.D. 25) Diethylphthalate 22.10 149 280 N.D. 26) 4- Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 29345.D GCMS1126.M Fri Dec 21 12:49:32 2001 Page 1

NYC-WTC 000036416

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000036416Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis comments, sample AD28967, Dec 2001 · Box DEP Box 22

NYC-WTC_000035607

Lab report noting bis(2-Ethylhexyl)phthalate detection and recovery issues in a water sample.

1 shared topics · Same agency, volume and box · similarity 0.998