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GCMS analysis comments, sample AD29089, December 2001

Machine-extracted title · confidence 88%

Analysis comments for sample AD29089 reporting no unusual compounds in GCMS scan but noting one compound recovery above acceptance range in LCS Standard.

NYC-WTC_000036000–000036009

Folder label: “GCMS X 11/30/01 A 12/11/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C: \HPCHEM\ 1 \DATA\DEC1001\29089.D Vial: 36 Acq On : 11 Dec 2001 10:48 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 15:33 2001 Quant Results File: GCMS1126 .RES: Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.03 178 113 N.D. 34) Anthracene 25.03 178 113 N.D. 35) Di-n-butylphthalate 26.99 149 26698 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.01 228 4371 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 12322 N.D. 43) Chrysene 33.01 228 4371 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.10 252 4405 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29089.D NP091101.M Mon Dec 17 15:26:21 2001 Page 2

NYC-WTC_000036003

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NYC-WTC_000036003Source: NYC Law Department, mirrored locally

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