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GCMS analysis comments, sample AD29025, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting detection of di-n-butylphthalate in sample AD29025 analyzed on December 18, 2001.

NYC-WTC_000035919–000035930

Folder label: “GCMS X 11/30/01 A 12/11/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1001\29025.D Vial: 29 Acq On : 11 Dec 2001 3:59 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 15:37 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 o' N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.03 178 900 N.D. 34) Anthracene 25.03 178 900 N.D. 35) Di-n-butylphthalate 26.99 149 52361 0.29 ug/1 98 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.49 149 174 N.D. 41) Benzo(a)anthracene 33.01 228 4100 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 9725 N.D. 43) Chrysene 33.01 228 4100 N.D. 45) Di-n-Octylphthalate 35.12 149 101 N.D. 46) Benzo(b)fluoranthene 36.12 252 451 N.D. 47) Benzo(k)fluoranthene 36.12 252 451 N.D. 4 8) Benzo(a)pyrene 37.10 252 5304 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29025.D NP091101.M Mon Dec 17 13:16:42 2001 Page 2

NYC-WTC_000035922

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NYC-WTC_000035922Source: NYC Law Department, mirrored locally

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