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Document / 11 pages

GCMS analysis comments, sample AD29138, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS scan results for sample AD29138 with no unusual compounds detected.

NYC-WTC_000035967–000035977

Folder label: “GCMS X 11/30/01 A 12/11/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\29138.D Vial: 38 Acq On : 12 Dec 2001 12:45 am Operator: 209 GALOS Sample : gc/ms scan 11/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.60 3.71 ug/1 1064790 1,4-Dichlorobenzene-d4 11.68 Hit# of 5 Tentative ID MW Mol Form CAS# Qual

1 Silane, tetramethyl - 88 C4H12Si 000075-76-3 32 2 N-Ethyl formami de 73 C3H7NO 000627-45-2 9 3 1,3 -Dioxolane, 2-pentadecyl- 284 C18H3602 004360-57-0 9 4 Pentane_3-methoxy­ 102 C6H140 036839-67-5 9 Abundance Scan 278 (7.599 mln): 29138.D (-) m/z 73.0,0 100.00% i 73 i ] 5000 43 • I ‘ ‘ ‘ ‘ 1 ‘ 1 ’ rl ’ ‘ * J • ■ । ■ 7.20 7.40 7.60 7.80 8.00 miz-> -L4 87 103 i j TTT TTTTTs iii TITT i । I ii ii । t i * » । » ii: । : TTT । (it » । ill l | ll 20 40 60 80 100 120 140 160 180 200 220 240 260 280 m/z 43.00 26.92% Abundance #62932: Silane, tetramethyl- 73

5000 1IIET T 1118 r I , -r-T-r-j-7 ■ > I 1 1 7.20 7.40 7.60 7.80 8.00 45 m/z 45.0,5 10.23% 15 J , 59 88 ■ i • ■ ■ • i 11:2111111111111 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #292: N-Ethylformamide 30 73 anmnnnTTeT 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.0.0 10.14% 44 58

15 a, l: . 1 j iV. . fl ’G1---ETTTSETrTr1PS_SI3ES-T5S ’1311471*4S*11*1TVII1*II7S8 miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #40191: 1,3-Dioxolane, 2-pentadecyl- "TTeTPTTTr 73 7.20 7.40 7.60 7.80 8.00 m/z 71.0,0 6.50% 5000

43 57 86 99 256 283 I t { 14 ( i TTT i TTT lit I I i t t | i 1 • / ( 111) j I 1 i I | > 1 I I j > I I i | 4 I I i | ) I I i | I Ji III TIT[T I T,-, . , , j I I I l'| I I I TIr T | I I miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 7.20 7.40 7.60 7.80 8.00

29138.D GCMS1126.M Wed Dec 12 15:55:39 2001 Page 1

NYC-WTC_000035974

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NYC-WTC_000035974Source: NYC Law Department, mirrored locally

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