GCMS analysis comments for sample AD29190, Dec 17 2001

Machine-extracted title · confidence 95%

Lab notes for sample AD29190 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.

NYC-WTC_000035843–000035852

Folder label: “GCMS X 11/30/01 A 12/10/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1001\29190.D Vial: 12 Acq On : 10 Dec 2001 9:28 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 15:07 2001 Quant Results File:.GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units.Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 951632 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3645523 20.00 ug/1 -0.03 17) Acenaphthene-dl0 20.55 164 1846504 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2602270 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1571883 20.00 ug/1 -0.02 44) Perylene-dl2 37.09 264 1082070 20.00 ug/1 -0.02

. System Monitoring Compounds 37) 2,4-DDD 30.05 235 167608 5.41 ug/mL -0.02 Spiked Amount 5.000 Recovery = 108.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.28 74 288 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 13.57 82 300 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 1109 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 20.57 153 113 N.D. 24) 2,4-Dinitrotoluene 20.96 165 209 N.D. 25) Diethylphthalate 22.08 149 2625 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 29190.D GCMS1126.M Thu Dec 13 09:17:58 2001 Page 1

NYC-WTC_000035845

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