Laboratory analysis notes for sample AD29023 indicating no unusual compounds detected in GCMS scan; one of forty-three compounds in quality control standard outside acceptance rang
NYC-WTC_000035808–000035819Folder label: “GCMS X 11/30/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC1001\29023.D Vial: 7 Acq On : 10 Dec 2001 4:35 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTBINT.P Quant Time: Dec 12 15:05 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 906375 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3483079 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 1754182 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.97 188 2517456 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1593597 20.00 ug/1 -0.03 44) Perylene-dl2 37.10 264 1101951 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 163813 5.47 ug/mL -0.02 Spiked Amount 5.000 Recovery = 109.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.20 74 304 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichiorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 1033 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.03 165 218 N.D. 25) Diethylphthalate 22.07 149 731 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 23.15 77 194 N.D.
(#) = qualifier out of range (m) = manual integration 29023.D GCMS1126.M Thu Dec 13 10:05:48 2001 Page 1
NYC-WTC_000035810
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NYC-WTC_000035820
Lab notes for sample AD29022 indicate no unusual compounds detected but one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035978
Laboratory report noting detection of di-n-butylphthalate in sample AD29026 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036103
Laboratory report noting GCMS scan results for sample AD29189 with di-n-butylphthalate detected and low pH.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036425
Laboratory report documenting GCMS analysis of sample AD29457 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036447
Laboratory report documenting GCMS analysis of sample AD29459 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035629
Lab report noting no unusual compounds but recovery issues in a water sample.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035955
Laboratory report documenting GCMS scan results for sample AD29137 with no unusual compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000035773
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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NYC-WTC_000035774
Laboratory data sheet recording sample volumes and drip rates for GCMS Method S08 analysis.
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NYC-WTC_000035776
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
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NYC-WTC_000035788
Calibration data sheet verifying instrument response for nitrosamines and benzene derivatives.
Filed in the same folder
NYC-WTC_000035793
Document containing reference values and recovery data for organic compounds analyzed by GCMS.
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