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GCMS analysis results, sample AD28903, Dec 2001

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GCMS analysis results for sample AD28903 dated December 15, 2001, showing non-detect levels for various compounds.

NYC-WTC_000035563–000035570

Folder label: “GCMS X 11/29/01 A 12/7/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC0 7 01\LB.D Vial: 7 Acq On 7 Dec 2001 8:47 pm Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 13 14:48 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether .0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.98 178 961 N.D. 34) Anthracene 24.98 178 961 N.D. 35) Di-n-butylphthalate 26.99 149 8978 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.49 149 2821 N.D. 41) Benzo(a)anthracene 33.01 228 4494 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 40712 0.41 ug/1 98 43) Chrysene 33.01 228 4494 N.D. 45) Di-n-Octylphthalate 35.04 149 627 N.D. 46) Benzo(b)fluoranthene 36.08 252 345 N.D. 47) Benzo(k)fluoranthene 36.13 252 586 N.D. 4 8) Benzo(a)pyrene 37.10 252 4856 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS1126.M Thu Dec 13 14:48:59 2001 Page 2

NYC-WTC_000035565

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NYC-WTC_000035565Source: NYC Law Department, mirrored locally

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GCMS blank analysis report, Feb 2002 · Box DEP Box 12

NYC-WTC_000005159

Blank sample analysis report confirming no contamination above method detection limits for target compounds analyzed on February 1, 2002.

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