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GCMS analysis comments for sample AD29141, Dec 17 2001

Machine-extracted title · confidence 95%

Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.

NYC-WTC_000035831–000035842

Folder label: “GCMS X 11/30/01 A 12/10/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C: \HPCHEM\ 1\DATA\DEC1001\29141.D Vial: 8 Acq On : 10 Dec 2001 5:34 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 15:17 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.03 178 528 N.D. 3 4) Anthracene 25.03 178 528 N.D. 35) Di-n-butylphthalate 26.99 149 36705 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 4 0) Butylbenzylphthalate 31.50 149 428 N.D. 41) Benzo(a)anthracene 33.00 228 3847 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 40218 0.45 ug/1 # 99 43) Chrysene 33.00 228 3847 N.D. 45) Di-n-Octylphthalate 35.06 149 730 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 36.11 252 215 N.D. 4 8) Benzo(a)pyrene 37.10 252 4079 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29141.D GCMS1126.M Thu Dec 13 10:14:10 2001 Page 2

NYC-WTC_000035834

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NYC-WTC_000035834Source: NYC Law Department, mirrored locally

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