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Document / 11 pages

GCMS analysis comments for sample AD28598, Dec 2001

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Laboratory report detailing GCMS scan results for sample AD28598, noting phthalate detection and recovery rates.

NYC-WTC_000034927–000034937

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV3001\28651.D Vial: 49 Acq On : 30 Nov 2001 2:41 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 30 15:31 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.14 65 187 N.D. 37) 2,4-Dinitrotoluene 21.01 165 289 N.D. 38) Diethylphthalate 22.09 149 659 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 25.06 178 369 N.D. 49) Anthracene 25.06 178 369 N.D. 50) Di-n-butylphthalate 27.01 149 12466 N.D. 51) Fluoranthene 28.70 202 787 N.D. ' 54) Pyrene 29.36 202 1086 N.D. 55) Butylbenzylphthalate 31.52 149 4524 N.D. 5 6) Benzo(a)anthracene 33.03 228 4322 N.D. 57) Bis(2-ethylhexyl)phthalate 33.31 149 12983 N.D. 58) Chrysene 33.11 228 799 N.D. 60) Di-n-Octylphthalate 35.04 149 1255 N.D. 61) Benz o(b)fluoranthene 36.09 252 607 N.D. 62) Benzo(k)fluoranthene 36.14 252 1130 N.D. 63) Benzo(a)pyrene 36.95 252 490 N.D. 64) Indenod, 2,3-cd) pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo (g, h, i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28651.D GCMS1126.M Fri Nov 30 16:41:46 2001 Page 2

NYC-WTC_000034929

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NYC-WTC_000034929Source: NYC Law Department, mirrored locally

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