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GCMS comments for sample AD28594, Dec 2001

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Laboratory analyst notes on GCMS scan results detecting bis(2-ethylhexyl)phthalate and recovery rates for sample AD28594.

NYC-WTC_000034750–000034758

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2901\28600.D Vial: 39 Acq On : 30 Nov 2001 12:20 am Operator: 209 GALOS Sample 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 30 14:48 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 20.96 165 389 N.D. 38) Diethylphthalate 22.10 149 386 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 24.98 178 563 N.D. 49) Anthracene 24.98 178 563 N.D. 50) Di-n-butylphthalate 27.00 149 14063 N.D. 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 0.00 149 0 N.D. 56) Benzo(a)anthracene 33.02 228 2899 N.D. 57) Bis(2-ethylhexyl)phthalate 33.30 149 4454 N.D. 58) Chrysene 33.02 228 2899 N.D. 60) Di-n-Octylphthalate 0.00 149 0 N.D. 61) Benzo(b)fluoranthene 0.00 252 0 N.D. 62) Benzo(k)fluoranthene 0.00 252 0 N.D. 63) Benzo(a)pyrene 37.13 252 2398 N.D. 64) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo (g, h, i) perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28600.D GCMS1126.M Fri Nov 30 14:49:04 2001 Page 2

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NYC-WTC_000034752Source: NYC Law Department, mirrored locally

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