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GCMS analysis comments for sample AD28596, Dec 2001

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Laboratory report detailing GCMS scan results for sample AD28596, noting phthalate detection and recovery rates.

NYC-WTC_000034919–000034926

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\NOV2901\28598 .D Vial: 47 Acq On : 30 Nov 2001 8:09 am Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 30 15:09 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 33) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 21.05 165 136 N.D. 3 8) Diethylphthalate 22.10 149 461 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 25.06 178 666 N.D. 49) Anthracene 25.06 178 666 N.D. 50) Di-n-butylphthalate 27.00 149 7245 N.D. ' 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 56) Benz o(a)anthracene 57) Bis(2-ethylhexyl)phthalate 58) Chrysene 60) Di-n-Octylphthalate 31.52 33.02 33.31 33.02 0.00 149 228 149 228 149 430 3090 92367 3090 0 C. N.D. 97

61) Benzo(b)fluoranthene 0.00 252 0 N.D. 62) Benzo(k)fluoranthene 0.00 252 0 N.D. 63) Benzo(a)pyrene 37.12 252 2894 ’ N.D. 64) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28598.D GCMS1126.M Fri Nov 30 15:42:21 2001 Page 2

NYC-WTC_000034921

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NYC-WTC_000034921Source: NYC Law Department, mirrored locally

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