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GCMS comments for sample AD28666, Dec 2001

Machine-extracted title · confidence 100%

Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.

NYC-WTC_000034819–000034829

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2901\28649.D Vial: 48 Acq On : 30 Nov 2001 9:38 am Operator: 209 GALOS Sample : 11/23 scan Inst S GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 30 15:13 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 33) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.13 65 1615 N.D. 37) 2,4-Dinitrotoluene 20.92 165 756 N.D. 38) Diethylphthalate 22.10 149 517 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 22.75 168 240 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 48) Phenanthrene 24.99 178 581 N.D. 49) Anthracene 24.99 178 581 N.D. 50) Di-n-butylphthalate 27.00 149 18485 N.D. 51) Fluoranthene 0.00 202 0 N.D. ‘ 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 31.50 149 201 N.D. 56) Benzo(a)anthracene 33.02 228 2779 N.D. 57) Bis(2-ethylhexyl)phthalate 33.30 149 4625 N.D. 58) Chrysene 33.02 228 2779 N.D. 60) Di-n-Octylphthalate 35.48 149 391 N.D. 61) Benzo(b)fluoranthene 36.15 252 199 N.D. 62) Benzo(k)fluoranthene 36.15 252 199 N.D. 63) Benzo(a)pyrene 37.12 252 3172 N.D. 64) Indeno(1,2,3-cd) pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28649.D GCMS1126.M Fri Nov 30 16:26:38 2001 Page 2

NYC-WTC_000034821

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NYC-WTC_000034821Source: NYC Law Department, mirrored locally

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