NYC-WTC_000035342
Log recording sample volume, drip rates, and addition details for GCMS analysis in December 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 8 pages
GCMS calibration table for TCLP analysis, Dec 2001
Machine-extracted title · confidence 95%Laboratory calibration table for EPA Method 625/TCLP analysis dated December 21, 2001, listing standard compounds and response factors.
NYC-WTC_000034428–000034435Folder label: “GCMS X 11/21/01 A 12/21/01”
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\DEC1901\LBC.D Vial: 23 Acq On : 21 Dec 2001 4:01 am Operator: GALOS Sample : gems unknown 11/21 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 21 9:27 2001 Quant Results File: NP112701.RES
Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.86 152 1033893 20.00 ng/uL -0.07 19) Naphthalene-d8 15.48 136 4145972 20.00 ng/uL -0.07 31) Acenaphthene-diO 20.75 164 1857277 20.00 ng/uL -0.07 49) Phenanthrene-diO 25.16 188 2702518 20.00 ng/uL -0.08 59) Chrysene-dl2 33.17 240 1825203 20.00 ng/uL -0.08 68) Perylene-dl2 37.25 264 924402 20.00 ng/uL -0.09
System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.85 132 737 0.01 ng/uL 0.43 Spiked Amount 75.000 Range 34 84 Recovery = 0.01%# 7) 1,2-Dichlorobenzene-d4 0.00 152 0 0.00 ng/uL Spiked Amount 50.000 Range 26 73 Recovery = 0.00%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 18.89 172 2201 0.02 ng/uL ।0.06 Spiked Amount 50.000 Range 42 78 Recovery = 0.04%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%#
Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2 -Chioropheno1 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis (1-Chioropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D.
(#) = qualifier out of range (m) = manual integration LBC.D NP112701.M Fri Dec 21 09:29:16 2001 Page 1
NYC-WTC_000034428
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NYC-WTC_000034428Source: NYC Law Department, mirrored locally
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