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GCMS comments for sample AD28469, Dec 2001

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Laboratory commentary dated December 3, 2001, regarding sample AD28469 analysis, noting bis(2-Ethylhexyl)phthalate presence.

NYC-WTC_000034376–000034383

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2901\28469.D Vial: 31 Acq On : 29 Nov 2001 3:32 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 29 16:21 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 0.00 65 0 N.D. 37) 2,4-Dinitrotoluene 20.94 165 408 N.D. 38) Diethylphthalate 22.09 149 470 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 22.71 77 109 N.D. 43) 4,6-Dinitro-2-methylphenol 22.44 198 2586 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 0.00 266 0 N.D. 4 8) Phenanthrene 24.99 178 739 N.D. 49) Anthracene 24.99 178 739 N.D. 50) Di-n-butylphthalate 27.01 149 11872 N.D. 51) Fluoranthene 28.72 202 374 N.D. 54) Pyrene 29.35 202 3010 N.D. 55) Butylbenzylphthalate 31.97 149 402 N.D. 5 6) Benz o(a)anthracene 33.02 228 2239 N.D. 57) Bis(2-ethylhexyl)phthalate 33.31 149 302 0135 55.32 ug/1 99 58) Chrysene 33.02 228 —2239 N.D. 60) Di-n-Octylphthalate 35.46 149 171 N.D. 61) Benzo(b)fluoranthene 36.07 252 219 N.D. 6 2) Benzo(k)fluoranthene 36.07 252 219 N.D. 63) Benzo(a)pyrene 37.11 252 2307 N.D. 64) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 65) Dibenz(a,h)anthracene 0.00 278 0 N.D. 66) Benzo (g, h, i) perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 28469.D NP112601.M Fri NOV 30 12:39:15 2001 Page 2

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