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GCMS analysis results for sample AD28269, Nov 2001

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Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.

NYC-WTC_000034180–000034197

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV2901\28263 .D Vial: 33 Acq On : 29 Nov 2001 6:28 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 30 9:58 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 33) Acenaphthylene 0.00 152 0 N.D. 3 4) Acenaphthene 0.00 153 0 N.D. 35) 2,4-Dinitrophenol 0.00 184 0 N.D. 36) 4-Nitrophenol 21.04 65 N.D. 37) 2,4-Dinitrotoluene 21.04 165 397— N.D. 38) Diethylphthalate 22.10 149 517 N.D. 39) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 40) Fluorene 0.00 166 0 N.D. 41) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 43) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 0.00 168 0 N.D. 45) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 46) Hexachlorobenzene 0.00 284 0 N.D. 47) Pentachlorophenol 4 8) Phenanthrene 0.00 25.06 266 178 0 437/ N.D. N.D. 49) Anthracene 25.06 178 437/ N.D. 50) Di-n-butylphthalate 27.00 149 9075, N.D. 51) Fluoranthene 0.00 202 0 N.D. 54) Pyrene 0.00 202 0 N.D. 55) Butylbenzylphthalate 31.50 149 658 N.D. 56) Benzo(a)anthracene 33.03 228 4815 N.D. 57) Bis(2-ethylhexyl)phthalate 33.30 149 5443 N.D. 58) Chrysene 33.10 228 2422 N.D. 60) Di-n-Octylphthalate 35.04 149 1292 N.D. 61) Benzo(b)fluoranthene 36.07 252 1089 N.D. 62) Benzo(k)fluoranthene 36.14 252 3014 N.D. 63) Benzo(a)pyrene 36.94 252 1358 N.D. 64) Indeno(1,2,3-cd)pyrene 40.83 276 3442 N.D. 65) Dibenz(a,h)anthracene 40.88 278 3529 N.D. 66) Benzo(g,h,i)perylene 41.92 276 5896 N.D.

(#) = qualifier out of range (m) = manual integration 28263.D NP112601.M Fri Nov 30 09:59:22 2001 Page 2

NYC-WTC_000034183

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NYC-WTC_000034183Source: NYC Law Department, mirrored locally

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