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GCMS analysis results for sample AD27955, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS analysis of sample AD27955 conducted on January 2, 2002.

NYC-WTC_000034111–000034123

Folder label: “GCMS X 11/20/01 A 12/20/01

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Scanned page image, NYC-WTC_000034117
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27955.D Vial: 11 Acq On : 21 Dec 2001 1:17 am Operator: GALOS Sample : gems unknown 11/20 Inst :'GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.472 173 178 184 rBV 101971 183371 1.73% 0.335% 2 6.573 184 189 199 rW 166243 356892 3.36% 0.652% 3 6.710 199 204 210 rW 79178 149271 1.40% 0.273% 4 6.820 211 216 223 rVB 107852 209932 1.98% 0.383% 5 7.838 323 327 340 rBV 787195 1507457 14.19% 2.752%

6 11.864 760 766 777 rVB 3873011 8118467 76.40% 14.822% 7 15.477 1152 1160 1177 rBV 4227428 10625889 100.00% 19.400% 8 20.750 1726 1735 1748 rBV 4322910 10288968 96.83% 18.785% 9 25.160 2206 2216 2226 rBV2 4119044 9876873 92.95% 18.032%' 10 25.298 2226 2231 2237 rVB 46164 115274 1.08% 0.210% 11 33.175 3080 3090 3100 rBV2 3298166 8143658 76.64% 14.868% 12 37.256 3525 3535 3546 rBV2 1859622 5197067 48.91% 9.488%

Sum of corrected areas: 54773119

27955.D NP112701.M Fri Dec 21 09:59:38 2001

NYC-WTC_000034117

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NYC-WTC_000034117Source: NYC Law Department, mirrored locally

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