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GCMS TCLP calibration table, Dec 2001

Machine-extracted title · confidence 95%

Calibration table for TCLP analysis listing retention times and response factors for standard compounds on December 20-21, 2001.

NYC-WTC_000034006–000034017

Folder label: “GCMS X 11/20/01 A 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1901\LBB.D Vial: 3 Acq On : 20 Dec 2001 5:58 pm Operator: GALOS Sample : gems unknown 11/20 Inst :*GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.475 170 178 183 rBV 122177 228648 2.20% 0.430% 2 6.576 183 189 193 rBV 218498 415225 4.00% 0.782% 3 6.704 198 203 210 rVB 105833 194506 1.87% 0.366% 4 6.814 210 215 224 rBV 142561 286493 2.76% 0.539% 5 7.841 322 327 341 rBV 660703 1337086 12.87% 2.517%

6 11.858 760 765 777 rVB 3858224 7878012 75.82% 14.831% 7 15.471 1151 1159 1176 rBV 4216244 10390920 100.00% 19.562% 8 20.753 1726 1735 1758 rBV 4136074 10038347 96.61% 18.898% 9 25.164 2207 2216 2226 rBV2 4189529 9495564 91.38% 17.876%' 10 25.292 2226 2230 2237 rVB2 45182 108060 1.04% 0.203% 11 33.169 3080 3089 3100 rBV2 3281243 7748434 74.57% 14.587% 12 33.417 3109 3116 3122 rBV 65088 132003 1.27% 0.249% 13 37.250 3526 3534 3548 rBV2 1751320 4865730 46.83% 9.160%

Sum of corrected areas: 53119028

LBB.D NP112701.M Fri Dec 21 10:00:57 2001

NYC-WTC_000034010

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NYC-WTC_000034010Source: NYC Law Department, mirrored locally

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