GCMS TCLP calibration table, Dec 2001

NYC 9/11 Public Portal Document

% Quantitation Report (QT Reviewed) */ Data File : C:\HPCHEM\l\DATA\DEC1901\LBB.D Vial: 3 Acq On : 20 Dec 2001 5:58 pm Operator : GALOS Sample Mise : gems unknown 11/20

MS Integration Params: RTEINT.P Quant Time: Dec 21 8:44 2001 38314Y Inst . : Multiplr:

Quant Results File: GC/MS Ins 1.00

NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.86 152 1258424 20.00 ng/uL -0.08 19) Naphthalene-d8 15.47 136 5072450 20.00 ng/uL -0.08 31) Acenaphthene-diO 20.75 164 2202381 20.00 ng/uL -0.07 49) Phenanthrene-diO 25.16 188 3290344 20.00 ng/uL -0.08 59) Chrysene-dl2 33.17 240 2296947 20.00 ng/uL -0.08 68) Perylene-d12 37.25 264 1215286 20.00 ng/uL -0.09

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.86 132 1037 0.01 ng/uL 0.44 Spiked Amount 75.000 Range 34 84 Recovery = 0.01%# 7) 1,2-Dichlorobenzene-d4 12.05 152 276 0.01 ng/uL -0.41 Spiked Amount 50.000 Range 26 73 Recovery = 0.02%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 18.89 172 2693 0.02 ng/uL 0.06 Spiked Amount 50.000 Range 42 78 Recovery = 0.04%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%#

Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichiorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D.

(#) = qualifier out of range (m) = manual integration LBB.D NP112701.M Fri Dec 21 09:49:26 2001 Page 1

NYC-WTC_000034006