Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
NYC-WTC_000033834–000033846Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV2 601\28155.D Vial: 11 Acq On 26 Nov 2001 8:29 pm Operator: 209 GALOS Sample 11/20 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.
38.03 1.05 ug/1 157527 Perylene-dl2 37.11
Hit# of/5 Tentative ID MW MolForm CAS# Qual 1 1,1,/1,5,7,7,7-Heptamethyl-3,3-bis (t 444 C13H40O5Si6 038147-00-1 38 2 3,6/Dioxa-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 32 3 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 22 4 2^-Dimethyl-3,4-bis(trimethylsilyl 311 C15H29NO2Si2 000000-00-0 12 Abundance Scan 3593 (38.032 min): 28155.D (-) m/z 73.00 100.00% 73 147 221 5000 281 355 37.80 38.00 38.20 38.40 41 . 96 117 TH’... —pm 193 2534 TmmTT1 327 1 401 42 m/z 147.00 72.86% m40.6Q 8Q m/z-> Abundance
5000
m/z-> 45 — 1 tp i 20140160180 200 220 240260 280 300 320 340 360 380 4(» 420 73 #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t
147
207 I.... I.J.1.1..I.... 1.... I. I../....1 40 60 80 100120140160180200220240260280300320340360380400420 267
I""!1 355 429
।" " ।■■■•।■' ■■ । ■ _A TfM11Ar 37.80 38.00 38.20 38.40 m/z 221.05 59.71%
Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221 ■ ■ 1 • ■
73 37.80 38 00 38.20 38.40 5000 m/z 281.00” 32.99%
m/z-> Abundance I"’ 'I 117 ................... 191
mmkmmmmmmmn 279
40 60 60 100120140160180 200 220 240 260 280 300 320 340 360 380 ^X) 420
73 #74103: T risiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
147 "A T T’r 37.80 38.00 38.20 38.40 m/z 354.95 25.85% 5000 281 45 369 LT‘‘1 — 117 T"TTIEETTTTTTT 207 249 . TT......... mr 1" 1 ।.... ।. I.. ।.... ।... j...j. A -A ■ ।•■।.... 11. m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 37.80 38.00 38.20 38.40
28155.D GCMS1126.M Tue NOV 27 12:58:15 2001 Page 3
NYC-WTC_000033842
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NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033752
Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034402
Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035700
Laboratory notes stating the GCMS scan of sample AD28901 revealed no unusual compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
Filed in the same folder
NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
Filed in the same folder
NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
Filed in the same folder
NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
Filed in the same folder