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GCMS analysis log for unknown compounds, Dec 2001

Machine-extracted title · confidence 100%

Log of GCMS analysis for sample AD27193 conducted on December 19, 2001, detecting other unknown compounds.

NYC-WTC_000032826–000032836

Folder label: “GCMS X 11/14/01 A 12/12/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\DEC1201\27193.D Vial: 4 Acq On 12 Dec 2001 6:02 pm Operator: GALOS Sample : gc/ms unknown 11/14 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.165 32 35 48 rVB 35299 77996 1.06% 0.205% 2 7.797 318 322 340 rVB 368624 783317 10.62% 2.060% 3 10.263 587 591 599 rVB 57239 104637 1.42% 0.275% 4 10.474 610 614 622 rVB 59747 115166 1.56% 0.303% 5 11.831 757 762 774 rBV 2907408 5739786 77.79% 15.096%

6 15.445 1150 1156 1170 rBV 3695738 7378380 100.00% 19.406% 7 20.717 1725 1731 1749 rBV 3542310 7128748 96.62% 18.750% 8 25.119 2205 2211 2223 rBV2 3147283 6832456 92.60% 17.970% 9 33.124 3077 3084 3104 rBV2 2495291 5304960 71.90% 13.953% 10 37.205 3519 3529 3548 rBV2 1749688 4555368 61.74% 11.981%

Sum of corrected areas: 38020814

27193.D NP112701.M Fri Dec 14 10:07:06 2001

NYC-WTC_000032832

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NYC-WTC_000032832Source: NYC Law Department, mirrored locally

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