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GCMS calibration table for TCLP analysis, Dec 2001

Machine-extracted title · confidence 100%

Calibration data sheet for GCMS analysis using TCLP method, listing standards and response factors from December 2001.

NYC-WTC_000032818–000032825

Folder label: “GCMS X 11/14/01 A 12/12/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\DEC1201\LB.D Vial: 2 Acq On 12 Dec 2001 4:13 pm Operator: GALOS Sample : gc/ms unknown 11/14 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.792 318 322 339 rVB 418506 948542 9.01% 1.784% 2 11.827 757 762 775 rBV 3880140 8242316 78.31% 15.500% 3 15.440 1150 1156 1171 rBV 5432775 10525137 100.00% 19.793% 4 20.712 1725 1731 1750 rBV 5030533 10359741 98.43% 19.482% 5 25.123 2205 2212 2223 rBV2 4665418 9742303 92.56% 18.320%

6 33.129 3077 3085 3103 rBV2 3411200 7252531 68.91% 13.638% 7 37.209 3520 3530 3542 rBV 2291771 6106676 58.02% 11.484%

Sum of corrected areas: 53177246

LB.D NP112701.M . Fri Dec 14 10:09:33 2001

NYC-WTC_000032822

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NYC-WTC_000032822Source: NYC Law Department, mirrored locally

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