GCMS analysis results for sample AD27113, Dec 2001

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Laboratory report documenting GCMS analysis of environmental sample AD27113 conducted on December 10, 2001.

NYC-WTC_000032678–000032687

Folder label: “GCMS X 11/9/01 A 12/5/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) ata File C:\HPCHEM\l\DATA\DEC0501\27113.D Vial: 13 cq On 5 Dec 2001 7:54 pm Operator: GALOS ample gc/ms unknown 11/13 Inst : GC/MS Ins ! X SC : Multiplr: 1.00 IS Integration Params: RTEINT.P ant Time: Dec 7 10:32 2001 Quant Results File: NP112701.RES ant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) itle : 208 625/TCLP calibration table ast Update : Wed Nov 28 15:33:44 2001 esponse via : Initial Calibration ataAcq Meth : NP112701

Irrnal Standards R.T. Qlon Response Cone Units Dev(Min) 1,4-Dichlorobenzene-d4 11.87 152 1171624 20.00 ng/uL -0.07 1 : Naphthalene-d8 15.47 136 4507678 20.00 ng/uL -0.08 2. Acenaphthene-dlO 20.76 164 2028725 20.00 ng/uL -0.07 _‘* Phenanthrene-diO 25.17 188 2792133 20.00 ng/uL -0.08 E Chrysene-dl2 33.17 240 1539217 20.00 ng/uL -0.08 C Perylene-dl2 37.25 264 1041854 20.00 ng/uL -0.09

Sy em Monitoring Compounds 2-Fluorophenol 0.00 112 0 0.00 ng/uL piked Amount 75.000 Range 18 42 Recovery = 0.00%# Phenol-d5 0.00 99 0 0.00 ng/uL •iked Amount 75.000 Range 19 32 Recovery = 0.00%# 2-Chlorophenol-d4 11.87 132 760 0.01 ng/uL 0.45 •iked Amount 75.000 Range 34 84 Recovery = 0.01%# 1,2-Dichlorobenzene-d4 12.13 152 878 0.02 ng/uL -0.33 ked Amount 50.000 Range 26 73 Recovery = 0.04%# Nitrobenzene-d5 0.00 82 0 0.00 ng/uL ked Amount 50.000 Range 55 98 Recovery = 0.00%# 3 2-Fluorobiphenyl 18.90 172 2284 0.02 ng/uL 0.07 'iked /Amount 50.000 Range 42 78 Recovery = 0.04%# 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL ■iked Amount 75.000 Range 45 96 Recovery = 0.00%# € Terphenyl-dl4 0.00 244 0 0.00 ng/uL ' il-ed Amount 50.000 Range 58 98 Recovery = 0.00%#

T? a Compounds Qvalue Pyridine 0.00 79 0 N.D. W-nitrosodimet hyl amine 0.00 74 0 N.D. Phenol 0.00 94 0 N.D. bis(2 - Chloroethyl)ether 0.00 93 0 N.D. 2. 2-Chlorophenol 0.00 128 0 N.D. 1,3-Dichlorobenzene 0.00 146 0 N.D. 1,4-Dichlorobenzene 0.00 146 0 N.D. 1 1,2-Dichlorobenzene 0.00 146 0 N.D. 2-Methylphenol 0.00 108 0 N.D. 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 1 3&4-Methylphenol 0.00 108 0 N.D. -Nit rosodi-n-propylamine 0.00 70 0 N.D. exachloroe thane 0.00 117 0 N.D. Witrchenzene 0.00 77 0 N.D. Isophorone 0.00 82 0 N.D.

(i = qualifier out of range (m) = manual integration 2' 3.D 22112701.M Fri Dec 07 10:44:08 2001 Page 1

NYC-WTC_000032680

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NYC-WTC_000032680Source: NYC Law Department, mirrored locally

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