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GCMS analysis results for sample AD27056, Dec 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of environmental sample AD27056 conducted on December 10, 2001.

NYC-WTC_000032648–000032657

Folder label: “GCMS X 11/9/01 A 12/5/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) 1 ta File C:\HPCHEM\l\DATA\DEC0501\27110.D Vial: 12 nq On 5 Dec 2001 7:00 pm Operator: GALOS .' ample gc/ms unknown 11/13 Inst : GC/MS Ins ; isc Multiplr: 1.00 3 Integration Params: RTEINT.P < ant Time: Dec 7 10:32 2001 Quant Results File: NP112701.RES fuant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) itle : 208 625/TCLP calibration table nnst Update : Wed Nov 28 15:33:44 2001 ' sponse via : Initial Calibration ataAcq Meth : NP112701

In rnal Standards R.T. Qlon Response Cone Units Dev(Min) 1,4-Dichlorobenzene-d4 11.86 152 1203440 20.00 ng/uL -0.08 1 Naphthalene-d8 15.47 136 4686486 20.00 ng/uL -0.08 2..; Acenaphthene-diO 20.76 164 2141657 20.00 ng/uL -0.07 4 Phenanthrene-d10 25.17 188 3074587 20.00 ng/uL -0.08 5 . Chrysene-dl2 33.17 240 1838977 20.00 ng/uL -0.08 6 Perylene-d12 37.25 264 1288814 20.00 ng/uL -0.08

Sy am Monitoring Compounds ■ , 2 - Fluorophenol 0.00 112 0 0.00 ng/uL : ‘.'iked Amount 75.000 Range 18 42 Recovery = 0.00%# Phenol-d5 0.00 99 0 0.00 ng/uL iked Amount 75.000 Range 19 32 Recovery 0.00%# 2-Chlorophenol-di 11.87 132 704 0.01 ng/uL 0.45 iked Amount 75.000 Range 34 84 Recovery = 0.01%# 1, 2 -ichlorobenzene-d4 12.13 152 601 0.01 ng/uL -0.33 ked Amount 50.000 Range 26 73 Recovery = 0.02%# N i t r ob e n z e n e - d 5 0.00 82 0 0.00 ng/uL iked mount 50.000 Range 55 98 Recovery = 0.00%# 2 - Fluorobiphenyl 18.90 172 2148 0.02 ng/uL 0.07 ed Amount 50.000 Range 42 78 Recovery = 0.04%# 3 : 2,4,6-Tribromophenol. 0.00 330 0 0.00 ng/uL •iked Amount 75.000 Range 45 96 Recovery = 0.00%# 6 , Terphenyl-dl4 0.00 244 0 0.00 ng/uL •iked Amount 50.000 Range 58 98 Recovery = 0.00%# Ta ■ et Coppounds Qvalue Pyridine 0.00 79 0 N.D. N-nitrosodimethylamine 0.00 74 0 N.D. Phenol 0.00 94 0 N.D. bis(2-Chloroethyl)ether 0.00 93 0 N.D. 1 2-Chlorophenol 0.00 128 0 N.D. 1,3-Dichlorobenzene 0.00 146 0 N.D. J 1,4-Dichlorobenzene 0.00 146 0 N.D. 1 1,2-Dichlorobenzene 0.00 146 0 N.D. 1 2 -Methylphenol 0.00 108 0 N.D. 1 2 , 2 1 -oxybis ( l-Chloropropan 0.00 45 0 N.D. 1 3&4-Methylphenol 0.00 108 0 N.D. 1 N-1itr o s od i-n-p r opylami ne 0.00 70 0 N.D. 1 Hexa chioroethane 0.00 117 0 N.D. nitrobenzene 0.00 77 0 N.D. l sonorone 0.00 82 0 N.D.

(4 = qualifier out of range (m) = manual integration 2'. 0.D 0112701.5] Fri Dec 07 10:35:58 2001 Page 1

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