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GCMS analysis results for sample AD27056, Dec 2001

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Laboratory report documenting GCMS analysis of environmental sample AD27056 conducted on December 10, 2001.

NYC-WTC_000032648–000032657

Folder label: “GCMS X 11/9/01 A 12/5/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) ata File C:\HPCHEM\1\DATA\DEC0501\27110.D Vial: 12 q On 5 Dec 2001 7:00 pm Operator: GALOS ample gc/ms unknown 11/13 Inst : GC/MS Ins SC : Multiplr: 1.00 ; Integration Params: RTEINT.P ant Time: Dec 7 10:32 2001 Quant Results File: NP112701.RES ant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) itle : 208 625/TCLP calibration table ast Update : Wed Nov 28 15:33:44 2001 sponse via : Initial Calibration MntaAcq Meth : NP112701

Compound R.T. QIon Response Cone Unit * Qvalue 2-Nitrophenol 0.00 139 0 N.D. 2,4-Dimethylphenol 0.00 107 0 N.D. 2 ; bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 2,4-Dichlorophenol 0.00 162 0 N.D. 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 2 Naphthalene 0.00 128 0 N.D. 2 Hexachlorobutadiene 0.00 225 0 N.D. 4-Chloro-3-methylphenol 0.00 107 0 N.D. 2 • Hexachlorocyclopentadiene 0.00 237 0 N.D. 2,4,6-Trichlorophenol 0.00 196 0 N.D. 3 2,4,5-Trichlorophenol 0.00 196 0 N.D. 7 2-Chloronaphthalene 0.00 162 0 N.D. Dimethylphthalate 0.00 163 0 N.D. 2,6-Dinitrotoluene 0.00 165 0 N.D. d 4 Acenaphthylene 0.00 152 0 N.D. 4 Acenaphthene 0.00 153 0 N.D. 4 , 2,4-Dinitrophenol 0.00 134 0 N.D. 4 4 -Ni trophenol 0.00 65 0 N.D. 4 2,4-Dinitrotoluene 0.00 165 0 N.D. 4 Diethylphthalate 0.00 149 0 N.D. 4 4 -Chlorophenylphenylether 0.00 204. 0 N.D. 4 Fluorene 0.00 166 0 N.D. 4 Azobenzen/ 1,2 -Diphenylhyd 0.00 77 0 N.D. C. 4,6- Dinitro- 2 -methylphenol 0.00 198 0 N.D. c N - N i t r o s o d i p h e ny l a m i n e 0.00 169 0 N.D. 4-Bromophenyl-phenylether 0.00 248 0 N.D. Hexa chloroben z ene 0.00 234 0 N.D. £ Pentachlorophenol 0.00 266 0 N.D. Phenanthrene 25.17 178 291 N.D. Anthracene 25.17 178 291 N.D. r Di-n -butylphthalate 27.17 149 2726 N.D. Fluoranthene 0.00 202 0 N.D. 6 3,3' -Dichlorobenzidine 0.00 252 0 N.D. C Benzidine 0.00 184 0 N.D. c Pyrene 0.00 202 0 N.D. ( Bu ty l b en zylph t ha l a t e 0.00 14 9 0 N.D. ( 3enzo(a)anthracene 3 3.17 228 3788 N.D. 3is(2-ethylhexyl)phthalate 33 . 43 14 9 4909 N.D. ( Chrysene 33.17 228 3788 N.D. ( Di-n-Octylphthalate 0.00 149 0 N.D. Benzo (b) fluoranthene 0.00 252 0 N.D.

(i = qualifier out of range (m) = manual integration 2'. .0.D JP112701.M Fri Dec 07 10:35:59 2001 Page 2

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