GCMS analysis results for sample AD27112, Dec 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0501\27112.D Vial: 14 Acq On 5 Dec 2001 8:48 pm Operator: GALOS Sample gc/ms unknown 11/13 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.84 3.60 ng/uL 1184650 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 59 2 2 -Pentanone, 4 -hydroxy-4-methyl- 116 C6H1202 000123-42-2 53 3 2 - Pent anone , 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 43 4 Acetic id, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 28 Abundance Scan 327 (7.841 min): 27112.D (-) m/ z 43.00 100.00% 43

5000 59

101 7.40 7.60 7.80 1.00 8 20__ .... .4 I • ' ' ' I ' ' ’ ' I ' i - I IT i । i TT , , । 53 , | 83 — m/z 59.10 46.05% m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 4b

J1 5000 59 7.40 7.60 7.80 8.00 8.20 m/z 58.10 16.80% 27 101 I | 49 :.... _ _ ■ ■ i • ■ ■ T i TI miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

7.40 7.60 7.80 8.00 8.20 5000 m/z 101.05 16.17% 59 4 101 15 31 83 I i ■ ■ ' ■ i ■ — ———————————————————— I miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245: 2-Pentanone, 4-hydroxy-4-methyl- 43 7.40 7.60 7.80 8.00 8.20 m/z 41.0 0 6.52% 5000- 59

31 101 । • ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■ l TI 4 |_____ 73 ' i ■ ■ • ■ i ■ • • 83 ■ i ■ > - -A -+s — m/z—> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 3.00 E.20

27112.D NP112701.M Fri Dec 07 12:57:29 2001 Page 1

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