GCMS analysis results for sample AD27290, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1201\27290.D Vial: 6 Acq On 12 Dec 2001 7:51 pm Operator: GALOS Sample : gc/ms unknown 11/14 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.80 3.13 ng/uL 967360 1,4-Dichlorobenzene-d4 11.84

Hit# of 5 Tentative ID/ MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 83 2 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 3 2-Pentanone, 4 -hydroxy-4 -methyl- 116 C6H1202 000123-42-2 43 4 Acetic acid, 1,1 dimethylethyl este 116 C6H12O2 000540-88-5 25 Abundance / Scan 323 (7.802 min): 27290.D (-) m/ z 43.10 100.00%| I < 43

5000 59

101 — 7.40 7.60 7.80 8.00 8.20 38,4 53.,. 1,1 ' I TT 69 1 I ' ■ ■ 1 i 83 1 T m/ Z 59.10 48.32% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.40 7.60 7.80 8.00 8.20 m/ z 58.10 19.67% 27 on 101 I l 49 . I 03 I ■ ■ i ■ ■ ' ■ i ' i 1 ' ■ ' i ' ' ' ' i .m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

7.40 7.60 7.80 8.00 8.20 5000- m/z 101.05 16.09% 59

15 31 101 83 — i ’ ■ ■ ■ i Im ■ ' ' i ■ ■ ■ ■ i ' ' ■ ■ i ' ' 1 1 I 1 1 1 1 I 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 'Abundance #3245: 2-Pentanone, 4-hydroxy-4-methyl- i 43 7.40 7.60 7.80 8.00 8.20 l m/z 41.10 7.04% 5000 59

miz- ------- 10 20 31

30 40 — 50 60 70 3 i • ■ ■ ■ i ’ ■ ■ ■ i • ■ • ■ i 1 1 1 1 TUT 80 90 100 । 1 1 1 110 i । Mr i t ) । । < i' i <• r > । j । । । । । t t

7.40 7.60 7.80 8.00 8.20

27290.D NP112701.M Fri Dec 14 10:09:25 2001 Page 1

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