GCMS analysis results for sample AD27112, Dec 2001

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Laboratory report documenting GCMS analysis of environmental sample AD27112 conducted on December 10, 2001.

NYC-WTC_000032668–000032677

Folder label: “GCMS X 11/9/01 A 12/5/01”

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NYC 9/11 Public Portal Document

{ Quantitation Report (QT Reviewed)

Da: 1 File C:\HPCHEM\l\DATA\DEC0501\27112.D Vial: 14 Ae 1 On 5 Dec 2001 8:48 pm Operator: GALOS Si ole gc/ms unknown 11/13 Inst : GC/MS Ins Mi . J : Multiplr: 1.00 M.:. Integration Params: RTEINT.P Quant Time: Dec 7 10:32 2001 Quant Results File: NP112701.RES

Qus it Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Tisle : 208 625/TCLP calibration table La - Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DamnAcq Meth : NP112701

Inte :al Standards R.T. Qlon Response Cone Units Dev(Min)

i: 4-Dichlorobenzene-d4 11.87 152 1065075 20.00 ng/uL -0.07 19: aphthalene-d8 15.48 136 4040826 20.00 ng/uL -0.07 31; cenaphthene-d10 20.75 164 1833297 20.00 ng/uL -0.07 4 9: henan t hrene - dl 0 25.16 188 2603364m 20.00 ng/uL -0.08 59: :rysene-d12 33.17 240 1579194 20.00 ng/uL -0.08 68) erylene-d12 3 7.26 264 1099423 20.00 ng/uL -0.08

Syst • i Monitoring Compounds 4) 3- Fluorophenol 0.00 112 0 0.00 ng/uL Sr ed Amount 75.000 Range 18 42 Recovery 0.00%# s: henol-d5 0 . 00 99 0 0.00 ng/uL S: ' ted Amount 75.000 Range 19 32 Recovery 0.00%# 6. 1-Chlorophenol-d4 11.87 132 683 0.01 ng/uL 0.44 S ■ -od Amount 75.000 Range 34 84 Recovery 0.01%# 7. , 2-Di chlorobenzene-d4 12.06 152 ■ 2354 0.05 ng/uL -0.40 S ad Amount 50.000 Range 26 73 Recovery = 0.10%# 20. itrobenzene-d5 0.00 82 0 0.00 ng/uL S’ ed Amount 50.000 Range 55 98 Recovery = 0.00%# 32, '.-Fluorobiphenyl 18.91 172 2413 0.02 ng/uL 0.08 S' ’ ted Amount 50.000 Range 42 78 Recovery = 0.04%# 33. , 4,6-Tribromophenol 0.00 330 0 0.00 ng/uL S; ' ".ed Amount 75.000 Range 4 5 96 Recovery = 0.00%# 62. ‘erphenyl -dl4 0.00 244 0 0.00 ng/uL S' ’ .ed Amount 50.000 Range 58 98 Recovery = 0.00%#

Tar ■ Compounds Qvalue 2 yridi ne 0.00 79 0 N.D. 3 -nitrosodimethylamine 0.00 74 0 N.D. 8 enol 0.00 94 0 N.D. 9' ■is ( 2 - Chloroethyl) ether 0.00 93 0 N.D. io: : - Chlorophenol 0.00 128 0 N.D. n: 3-Dichlorobenzene 0.00 146 0 N.D. 12. 4-Dichlorobenzene 0.00 146 0 N.D. 13 .,2-Dichlorobenzene 0.00 146 0 N.D. 14 -Methylphenol 0.00 103 0 N.D. 15 , 2 1 -xybis (1-Chloropropan 0.00 45 0 N.D. 16 &4 -Methylphenol 0.00 108 0 N.D. 17 -Nitrosodi-n-propylamine 0.00 70 0 N.D. 18 exachloroethane 0.00 117 0 N.D. 21 itrohenzene 0.00 77 0 N.D. ophcrone 0.00 82 0 N.D.

(45) qualifier out of range (m) = manual integration 2 71’ 2 D NP112701.M Fri Dec 07 10:44:22 2001 Page 1

NYC-WTC_000032670

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NYC-WTC_000032670Source: NYC Law Department, mirrored locally

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GCMS results log, sample AD27110, Dec 10 2001 · Box DEP Box 21

NYC-WTC_000032638

Laboratory report for GCMS analysis of sample AD27110 completed on December 10, 2001.

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