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GCMS results log, sample AD27110, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27110 completed on December 10, 2001.

NYC-WTC_000032638–000032647

Folder label: “GCMS X 11/9/01 A 12/5/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

D- File C : \HPCHEM\l\DATA\DEC0501\27056 .D Vial: 15 A On 5 Dec 2001 9:43 pm Operator: GALOS Si le gc/ms unknown 11/13 Inst : GC/MS Ins M Multiplr: 1.00 M. ntegration Params: RTEINT.P Q : Time: Dec 7 10:33 2001 Quant Results File: NP112701.RES

Q‘ X Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) T. : 208 625/TCLP calibration table Lr Update : Wed Nov 28 15:33:44 2001 Re onse via : Initial Calibration D: ACq Meth : NP112701

Inti nl Standards R.T. Qlon Response Cone Units Dev(Min)

1 .4-Dichlorobenzene-d4 11.87 152 1028779 20.00 ng/uL -0.06 19 phthalene-d8 15.49 136 3856383 20.00 ng/uL -0.06 31 enaphthene-d10 20.76 164 1755744 20.00 ng/uL -0.06 49 enanthrene-dl0 25.17 188 2564019m 20.00 ng/uL -0.07 59 •rysene-dl2 33 . 17 240 1635727 20.00 ng/uL -0.07 68 rylene-d12 37.26 264 1139844 20.00 ng/uL -0.07

Sys Monitoring Compounds 4 - Fluorophenol 0.00 112 0 0.00 ng/uL S’ 2d Amount 75.000 Range 18 42 Recovery = 0.00%# 5 enol-d5 0.00 99 0 0.00 ng/uL S d Amount 75.000 Range 19 32 Recovery = 0.00%# 6 ..Chlorephenol-d4 11.86 132 845 0.01 ng/uL 0.44 d An:ou? 75.000 Range 34 84 Recovery = 0.01%# . 2-Dich] robenzene-d4 12.18 152 322 0.01 ng/uL -0.28 C :d Amour 50.000 Range 26 73 Recovery = 0.02%# 20 croben 2 one - d5 0.00 82 0 0.00 ng/uL C :d Amo;int 5 0.000 Range 55 98 Recovery = 0.00%# 32. -Fluorobiphenyl 18.92 172 18 85 0.02 ng/uL 0.08 C 33 Amount 50.000 Range 42 78 Recovery = 0.04%# 33 , 4, 6-Tribromophenol 0.00 330 0 0.00 ng/uL S' d Amount 75.000 Range 4 5 96 Recovery = 0.00%# 62 rphenyl-d14 0.00 244 0 0.00 ng/uL c .d Amount 50.000 Range 53 98 Recovery = 0.00%#

Tar Compor n2s Qvalue ridin: 0.00 79 0 N.D. -itros r imethylamine 0.00 74 0 N.D. 8 enol 0.00 94 0 N.D. Q s (2-Chloroethy1) ether 0.00 93 0 N.D. 10 -Chlore h e n o l 0.00 128 0 N.D. 11 . 3 -Dichlorobenzene 0.00 146 0 N.D. 12 . 4 -Dicb. l orobenzene 0.00 146 0 N.D. 13 2 -Dichlorobenzene 0.00 146 0 N.D. 14 - let hyl phenol 0.00 108 0 N.D. 15 2 1 -cxyhis (1-Chloropropan 0.00 45 0 N.D. 16 14-MethyIphenol 0.00 108 0 N.D. 17 itror ■ ■ i-n-propylamine 0.00 70 0 N.D. 18 cachl- itethane 0.00 117 0 N.D. 21 0.00 77 0 N.D. 22 pphoro: 0.00 82 0 N.D.

(#) ralifi out of range (m) = manual integration 271 NP1.201 .M Fri Dec 07 10:44:38 2001 Page 1

NYC-WTC_000032640

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NYC-WTC_000032640Source: NYC Law Department, mirrored locally

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