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GCMS analysis results for sample AD27111, Dec 2001

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Laboratory report documenting GCMS analysis of environmental sample AD27111 conducted on December 10, 2001.

NYC-WTC_000032658–000032667

Folder label: “GCMS X 11/9/01 A 12/5/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C : \HPCHEM\1\DATA\DEC0501\27111 .D Vial: 11 7 cq On 5 Dec 2001 6:05 pm Operator: GALOS :! amp l e gc/ms unknown 11/13 Inst : GC/MS Ins rise : Multiplr: 1.00 1:3 Integration Params: RTEINT.P quant Time: Dec 7 10:31 2001 Quant Results File: NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : MP112 7 01

Compound R.T. Qlon Response Cone Unit Qvalue

2? 2 -Nitrophenol 0.00 139 0 N.D. 2-) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis (2-Chloroethoxy ) methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 2'; 1, 2 , 4-Trichlorobenzene 0.00 180 0 N.D. 2c ) Naphthalene 0.00 128 0 N.D. 25 ' Hexachlorobutadiene 0.00 225 0 N.D. 30) 4 - Chloro-3 -methylphenol 0.00 107 0 N.D. 34 ) Hexachlorocyclopentadiene 0.00 237 0 N.D. 3!) 2,4 , 6 -Trichlorophenol 0.00 196 0 N.D. 30) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 3”; 2-Chloronaphthalene 0.00 162 0 N.D. 3 ' Dimethylphthalate 0.00 163 0 N.D. 3’ .. 2 , 6-Dinitrotoluene 0.00 165 0 N.D. d 4' ) Acenaphthylene 0.00 152 0 N.D. 4: ) Acenaphthene 0.00 153 0 N.D. 4: ) 2,4-Dinitrophenol 0.00 184 0 N.D. 4: । 4-Nitrophenol 0.00 65 0 N.D. 4- ’ 2,4-Dinitrotoluene 0.00 165 0 N.D. 4:) Diethylphthalate 0.00 149 0 N.D. 40 ; 4-Chlorophenylphenylether 0.00 204 0 N.D. 4' ) Fluorene 0.00 166 0 N.D. 4: ) Azobenzen/ 1, 2 -Diphenylhyd 0.00 77 0 N.D. 5'; 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51: N-Nitrosodiphenylamine 0.00 169 0 N.D. 5: : 4-Bromophenyl-phenylether 0.00 248 0 N.D. 5.' ) Hexachlorobenzene 0.00 284 0 N.D. 5- .■ Pentachlorophenol 0.00 266 0 N.D. 5: ) Phenanthrene 25.17 17 8 287 N.D. 5: ! Anthracene 25.17 178 287 N.D. 5' ' Di-n-butylphthalate 27.16 149 9407 N.D. 5 : Fluoranthene 0.00 202 0 N.D. 6 i 3,31-Dichlorobenzidine 0.00 252 0 N.D. 6' ’ Benzidine 0.00 184 0 N.D. 6 : Pyrene 0.00 202 0 N.D. 6 Bucylbenzylphthalate 0.00 149 0 N.D. 6: ■ Benzo(a)anthracene 33.17 228 4501 N.D. 6 ■ Bis(2 - ethylhexyl)phthalate 3 3.43 149 14390 N.D. 6' i Chrysene 33.17 228 4501 N.D. 6: ) Di-n-Octylphthalate 0.00 149 0 N.D. 7:) Benzo (b) f luoranthene 0.00 252 0 N.D.

(4: = qualifier out or range (m) = manual integration 2011.D NP112701.M Fri Dec 07 10:35:46 2001 Page 2

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