GCMS analysis results for sample AD27111, Dec 2001

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Laboratory report documenting GCMS analysis of environmental sample AD27111 conducted on December 10, 2001.

NYC-WTC_000032658–000032667

Folder label: “GCMS X 11/9/01 A 12/5/01”

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NYC 9/11 Public Portal Document I '

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC0501\27111.D Vial: 11 2.cq On 5 Dec 2001 6:05 pm Operator: GALOS Sample gc/ms unknown 11/13 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 10:31 2001 Quant Results File: NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 response via : Initial Calibration TataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

") 1,4-Dichlorobenzene-d4 11.86 152 1300107 20.00 ng/uL -0.07 15) Naphthalene-d8 15.48 136 5060513 20.00 ng/uL -0.07 31) Acenaphthene-diO 20.76 164 2265587 20.00 ng/uL -0.06 4r) Phenanthrene-diO 25.17 188 3203567 20.00 ng/uL -0.07 5) Chrysene-dl2 33.17 240 1927372 20.00 ng/uL -0.07 6.) Perylene-d12 37.26 264 1310490 20.00 ng/uL -0.08

Sytem Monitoring Compounds •) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# :) Phenol-d5 0.00 99 0 0.00 ng/uL “oiked .Amount 75.000 Range 19 32 Recovery = 0.00%# 2-Chlorophenol-dl 11.86 132 1118 0.01 ng/uL 0.44 fiked Amount 75.000 Range 34 84 Recovery = 0.01%# ' ). 1, 2-Dichlorobenzene-d4 12.15 152 585 0.01 ng/uL -0.31 piked Amount 50.000 Range 26 73 Recovery = 0.02%# 2'J Nitrobenzene-d5 0.00 82 0 0.00 ng/uL piked Amount 50.000 Range 55 98 Recovery = 0.00%# 3' ) 2 - Fluorobiphenyl 13.90 172 2186 0.02 ng/uL 0.06 liked Amount 50.000 Range 42 78 Recovery = 0.04%# 3’) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL . iked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL S iked Amount 50.000 Range 58 98 Recovery = 0.00%#

Target Compounds Qvalue. 2.) Pyridine 0.00 79 0 N.D. 2 ) N-nitrosodimethylamine 0.00 74 0 N.D. 1) Phenol 0.00 94 0 N.D. !) bis ( 2 -Chloroethyl) ether 0.00 93 0 N.D. l' 2-Chlorophenol 0.00 128 0 N.D. 1’) 1,3-Dichlorobenzene 0.00 146 0 N.D. 1: ) 1,4-Dichlorobenzene 0.00 146 0 N.D. 1.1 1,2-Dichlorobenzene 0.00 146 0 N.D. 1- ) 2 -Methylphenol 0.00 108 0 N.D. IL) 2 , 21-oxybis(1-Chloropropan 0.00 45 0 N.D. KA 3 &4- Methylphenol 0.00 108 0 N.D. 17 ) N-?i crosodi-n - propylamine 0.00 70 0 N.D. IS ) Hexachloroethane 0.00 117 0 N.D. 22' Nitrobenzene 0.00 77 0 N.D. 2: ;■ Isophorone 0.00 82 0 N.D.

(#) = qualifier out of range (m) = manual integration 27'. 11. D ‘ P112701 .21 Fri Dec 07 10:35:45 2001 Page 1

NYC-WTC_000032660

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