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GCMS results log, sample AD26993, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26993 completed on December 11, 2001.

NYC-WTC_000032492–000032502

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File C:\HPCHEM\l\DATA\DEC0601\26993.D Vial: 27 Acq On 7 Dec 2001 10:44 am Operator: GALOS Sample g c/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.050 16 23 28 rVB 104886 199141 2.01% 0.386% 2 6.591 187 191 201 rW 60737 137867 1.39% 0.267% 3 7.856 325 329 347 rVB 626994 1277152 12.89% 2.474% 4 11.882 763 768 789 rVB 3665625 7903991 79.78% 15.308% 5 15.495 1156 1162 1180 rBV 4542024 9907410 100.00% 19.188%

6 20.777 1731 1738 1752 rBV 4560981 9767199 98.58% 18.917% 7 25.187 2212 2219 2231 rBV2 4269683 9248234 93.35% 17.912% 8 25.325 2231 2234 2247 rVB 35034 101461 1.02% 0.197% 9 33.184 3085 3091 3112 rBV2 3144744 7123063 71.90% 13.796% 10 37.274 3530 3537 3558 rBV2 2105672 5967115 60.23% 11.557%

Sum of corrected areas: 51632633

26993.D NP112701.M Tue Dec 11 14:55:35 2001

NYC-WTC_000032498

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NYC-WTC_000032498Source: NYC Law Department, mirrored locally

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