GCMS calibration table for TCLP analysis, Dec 6 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC0601\LBB.D —A n Vial: 14 Acq On 6 Dec 2001 10:00 pm (823 268) Operator: GALOS Sample lab blank 11/8 P /o Inst : GC/MS Ins Mise MS Integration Params: RTEINT.P 00 21601—3 Multiplr: 1.00

Quant Time: Dec 11 11:37 2001 L. A Quant Results File: NP112701.RES 200 - 17031 Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.89 152 1205687 20.00 ng/uL -0.05 19) Naphthalene-d8 15.50 136 4604078 20.00 ng/uL -0.05 31) Acenaphthene-d.10 20.77 164 2099779 20.00 ng/uL -0.05 49) Phenanthrene-diO 25.18 188 3055515 20.00 ng/uL -0.06 59) Chrysene-dl2 33.19 240 1992675 20.00 ng/uL -0.06 68) Perylene-dl2 37.28 264 1417144 20.00 ng/uL -0.06

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.89 132 429 0.01 ng/uL 0.46 Spiked Amount 75.000 Range 34 84 Recovery = 0.01%# 7) 1,2-Dichlorobenzene-d4 12.23 152 295 0.01 ng/uL -0.23 Spiked Amount 50.000 Range 26 73 Recovery = 0.02%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 18.92 172 2368 0.02 ng/uL 0.09 Spiked Amount 50.000 Range 42 78 Recovery = 0.04%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%#

Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D.

(#) = qualifier out of range (m) = manual integration LBB. D NP112701.M Tue Dec 11 14:27:09 2001 Page 1

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