GCMS analysis results for sample AD26830, Dec 11 2001

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Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\DEC2 101\26830.D Vial: 22 Acq On : 23 Dec 2001 5:14 am Operator: 209 GALOS Sample : gc/ms scan 12/17 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.57 2.99 ug/1 686671 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 47 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Butane, 2-methoxy-2-methyl-______ 102 C6H140 000994-05-8 9 Abundance Scan 275 (7.572 min): 26830.D (-) m/ z 73.00 1 00.00% 73

5000- 43

7.20 7.40 7.60 7.80 8.00 3? |, | 50 55 67, । । 87 103 'r' 11 1 1 1 ''1 1 1 1 '1 1 m/ z 43.00 30.35% m/z-> 10 20 30 40 50 60 70

C 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 TTToru ————— 7.20 7.40 7.60 7.80 8.00 45 m/ z 15 | 53 59 l............. 88............................. m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

7.20 7.40 7.60 7.80 8.00 | 5000 m/ z 41.05 10.96% 55 45 87 27 39 "ir ■ i ■ ■ ■ ■ i ■ ' I ' ’ ' ' I ' ' ' ' I T-»—r-r—-i i । i m/z->10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 7.20 7.40 7.60 7.80 8.00 73 m/ z 71.00 6.59% 5000 - 44 58 15 ' ■ i • ' ' ' i ' ' TTfrr m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 17.60 7.80_ 8.00

26830.D GCMS1126.M Fri Dec 28 15:04:37 2001 Page 1

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