Calibration data sheet listing standard compounds and response factors used for GCMS analysis on December 5, 2001.
NYC-WTC_000032142–000032159Folder label: “GCMS X 11/7/01 A 12/6/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File C:\HPCHEM\l\DATA\DEC0501\26712.D Vial: 3 Acq On 5 Dec 2001 10:35 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 7 9:55 2001 Quant Results File: NP112701.RES Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.86 152 1131948 20.00 ng/uL -0.08 19) Naphthalene-d8 15.47 136 4229441 20.00 ng/uL -0.08 31) Acenaphthene-diO 20.75 164 1885261 20.00 ng/uL -0.08 49) Phenanthrene-diO 25.17 188 2548107 20.00 ng/uL -0.08 59) Chrysene-dl2 33.16 240 1408776 20.00 ng/uL -0.09 68) Perylene-dl2 37.25 264 906689 20.00 ng/uL -0.09
System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 11.19 99 3 03 0.00 ng/uL 0.06 Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.87 132 1023 0.01 ng/uL 0.45 Spiked Amount 75.000 Range 34 84 Recovery = 0.01%# 7) 1,2-Dichlorobenzene-d4 12.16 152 557 0.01 ng/uL -0.30 Spiked Amount 50.000 Range 26 73 Recovery = 0.02%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 18.89 172 1602 0.01 ng/uL 0.06 Spiked Amount 50.000 Range 42 78 Recovery = 0.02%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%# Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 12.86 45 1603 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration 26712.D NP112701.M Fri Dec 07 09:58:59 2001 Page 1
NYC-WTC_000032142
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NYC-WTC_000031989
Laboratory report documenting GCMS analysis of sample AD26677 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031968
Laboratory report documenting GCMS analysis of sample AD26676 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032245
Gas chromatography-mass spectrometry analysis of sample AD26832 documenting unknown compounds with reference to comments.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031333
Laboratory report documenting GCMS analysis of sample AD26321 with unidentified compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032007
Laboratory report documenting GCMS analysis of sample AD26678 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031384
Report documenting GCMS analysis of sample AD26336 with a note regarding unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031415
Report documenting GCMS analysis of sample AD26386 with a note regarding unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032093
Laboratory report documenting GCMS analysis of sample AD26682 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031530
DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26392 noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031491
Laboratory comment confirming detection of Butylbenzylphthalate in sample AD26390 on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031889
GC/MS analysis of sample AD26538 identified other unknown compounds noted in comments section, December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032058
Laboratory report documenting GCMS analysis of sample AD26680 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000031869
Illegible text on a single page from the GCMS folder covering November to December 2001.
Filed in the same folder
NYC-WTC_000031870
Index or cover sheet page for the GCMS folder covering the period from November 7 to December 6, 2001.
Filed in the same folder
NYC-WTC_000031876
Calibration table listing standards like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 for GC/MS analysis dated December 2001.
Filed in the same folder
NYC-WTC_000031889
GC/MS analysis of sample AD26538 identified other unknown compounds noted in comments section, December 10, 2001.
Filed in the same folder
NYC-WTC_000031905
Laboratory report documenting GCMS analysis of sample AD26624 identifying unknown compounds on December 10, 2001.
Filed in the same folder