GCMS analysis results for sample AD26676, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26676.D Vial: 9 Acq On 6 Dec 2001 5:28 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Hexanone Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

6.46 0.46, ng/uL 142481 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hex.anone 100 C6H120 000589-38-8 90 2 3-Hexanone 100 C6H120 000589-38-8 90 3 3-Hexanone 100 C6H120 000589-38-8 72 4 Butane , 2,2-dimethyl- 86 C6H14 000075-83-2 59 Abundance Scan 177 (6.463 min): 26676.D (-) m/ z 43.05 100.00% 43 57

71 5000 - 100 39 6.20 6.40 6.60 6.80 mm — + 'I............ ‘I ■ ■«i»।" ।" >«। +11 ।.. ।।. i । i j ’i m/z 57.10 90.47% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Abundance #1528: 3-Hexanone 43 57

29 71 5000 6.201__ 6.40 6.60 6.80 100

L m/ 71.05 53.21% TTTTTTTT ...... I' '' 11TTTT ■*i ■’■ ■ i■ " r •' • i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 +85 m/z-> Abundance #63358: 3-Hexanone 43 57 1 ■ i ' 6.20 6.40 6.60 6.80 71 m/z 100.05 29.94% 5000 100 85 I I > I < I I O I I | I I I I | I I I I | I I < I | ■ 1′11′111000—111171711 T" ' 1 T‘ " ' I ' ‘TTyrm-j- m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63356: 3-Hexanone 1 i 29 43 57 6.20 6.40 6.60 6.80 i m/z 41.05 26.01% 5000- 71

100

m/z- " ' r " ' i' .. 38—4 ... prrort 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 I' ’ " I " •' I +85 T1" 11 AAAAA6.20 6.40 6.60 6.80

. 26676.D NP112701.M Fri Dec 07 14:51:30 2001 Page 5

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