GCMS calibration table for TCLP analysis, Dec 2001

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Calibration table listing standards like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 for GC/MS analysis dated December 2001.

NYC-WTC_000031876–000031888

Folder label: “GCMS X 11/7/01 A 12/6/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report s Data File C:\HPCHEM\1\DATA\DEC0 601\LBA.D Vial: 10 Acq On 6 Dec 2001 6:23 pm Operator: GALOS Sanpl e gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Ethane, 1,1,2,2-tetrachloro- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 9.64 2.90 ng/uL 740203 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethane, 1,1,2,2-tetrachloro- 166 C2H2C14 000079-34-5( 95 2 Ethane, 1,1,2,2-tetrachloro- 166 C2H2C14 000079-34-5 64 3 Ethane, 1,2,2-trichloro-1,1-difluor 168 C2HC13F2 000354-21-2 45 4 Ethane, 1,l-dichloro-2,2-difluoro- 134 C2H2C12F2 000471-43-2 42 Abundance Scan 523 (9.635 min): LBA.D (-) m/z 82.95 100.00% 83

5000

95 ...

miz-? 37 47 §1 —It...... — ■ i 73 ■ i ‘ 30 40 50 60 70 80 1.... 11 TOPIT 168 90 100 110 120 130 140 150 160 170 9.20 m/z 9.40 84.95 9.60 9.80 10.00 65.88% Abundance #13774: Ethane, 1,1,2,2-tetrachloro- 83

5000 i 1 1 ■ ■ i ■ ■ ■ • i • ‘ 'T 1 r 1 ■ 1 1 i ' 1 9.20 9.40 9.60 9.80 10.00 m/z 94.9, 14.29% 35 47 ; , 95 131 168 miz-> < ■ । ।' i i 1111 > 11 ‘ " 11'. 11 > — 4 ------- 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #37919: Ethane, 1,1,2.2-tetrachloro 83 9.20 9.40 9.60 9.80 10.00 '

"7. 5000

35 47 60 t 96 131 168 * * 1 ‘ ‘'i ' 1 * * i ‘ I *» ' 1 I ‘ * 1 * > < * I < » < » । i * <» । < i i i | i i i | | 1 > TTTTT i r| n ri| i i > 11 n in i i i i । m/z-? 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #68054: Ethane, 1,2,2-trichloro-1,1-difluoro- TI —6—G/O—nnim 188 TInr 83 9.20 9.40 9.60 9.80 10.00 'm/z 11.22% 5000 133 | 98 114 ..........I................ 168 —30354 — -HP 11 * i * ‘ । * ‘ * * । '"11111111. i> 111. i ■ i ■ *' • i ‘ “ 111 ■ ‘ । ■ 111 ■ m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 9.20 10.00

LBA.D NP112701.M Wed Dec 19 13:08:56 2001 Page 6

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